The C-glycosidic analogue of α-L-rhamnose 1-phosphate has been stereoselectively synthesised reacting 2,3,4-tri-O-benzyl-L-rhamnopyranose with tetraethyl methylenediphosphonate and sodium hydride in diglyme, and then deprotecting with iodotrimethylsilane.
Cipolla, L., LA FERLA, B., Nicotra, F., Panza, L. (1997). Easy and Stereoselective Synthesis of the Phosphono Analogue of a-L-Rhamnose 1-phosphate. TETRAHEDRON LETTERS, 38(31), 5567-5568 [10.1016/S0040-4039(97)01245-8].
Easy and Stereoselective Synthesis of the Phosphono Analogue of a-L-Rhamnose 1-phosphate
CIPOLLA, LAURA FRANCESCA;LA FERLA, BARBARA;NICOTRA, FRANCESCO;
1997
Abstract
The C-glycosidic analogue of α-L-rhamnose 1-phosphate has been stereoselectively synthesised reacting 2,3,4-tri-O-benzyl-L-rhamnopyranose with tetraethyl methylenediphosphonate and sodium hydride in diglyme, and then deprotecting with iodotrimethylsilane.
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