A simple, efficient, and general method for the synthesis of glycosyl phosphorothioate through a one-pot reaction of glycosyl bromide with diethyl phosphite, ammonium acetate, and sulphur in the presence of alumina under solvent-free conditions using microwave irradiation has been developed.
Cipolla, L., Redaelli, C., Faria, I., Nicotra, F. (2006). Easy access to glycosyl phosphorothioates with microwaves technique. JOURNAL OF CARBOHYDRATE CHEMISTRY, 25(2-3), 163-171 [10.1080/07328300600732204].
Easy access to glycosyl phosphorothioates with microwaves technique
CIPOLLA, LAURA FRANCESCA;NICOTRA, FRANCESCO
2006
Abstract
A simple, efficient, and general method for the synthesis of glycosyl phosphorothioate through a one-pot reaction of glycosyl bromide with diethyl phosphite, ammonium acetate, and sulphur in the presence of alumina under solvent-free conditions using microwave irradiation has been developed.
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